Spider-Man - Season 3 - Eps 18: Specialists and Slaves
An old enemy of Spidey's, a radiation specialist who once lifted Manhattan into the sky, has been released from jail and promptly revisits Manhattan's nuclear power plant, stuns the outdoor guards with his ray gun, and again commandeers the reactor.
About Spider-Man

Title: Spider-Man
First Air Date: 1967-09-09
Last Air Date: 1970-06-14
Status: Ended
Rating: 7.692/10 (from 195 votes)
Language: EN
Seasons: 3
Total Episodes: 77
Network: ABC Syndication
Genres: Kids, Animation, Action & Adventure
Production Companies: Grantray-Lawrence Animation, Krantz Animation
Synopsis
The bite of a radioactive spider transforms a teen into a superhero.
Cast

Bernard Cowan
Narrator (voice)

Paul Soles
Peter Park / Spider-Man (voice)

Paul Kligman
J. Jonah Jameson (voice)

Peg Dixon
Mary Jane Watson / May Parker / Betty Brant (voice)

Billie Mae Richards
Paperboy (voice) (uncredited)

Corinne Conley

Larry D. Mann

Len Carlson
Green Goblin (voice) (uncredited)